Technology Process of C35H53NO12S
There total 7 articles about C35H53NO12S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 10h;
DOI:10.1016/j.tetlet.2012.02.090
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 20 % Pd(OH)2/C; hydrogen / benzene / 10 h / 20 °C
2: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C
3: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran / 3 h / -78 - 20 °C
4: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / 10 h / -78 - 20 °C
With
1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; 20 % Pd(OH)2/C; hydrogen; iodine; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; benzene;
DOI:10.1016/j.tetlet.2012.02.090
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C
2: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran / 3 h / -78 - 20 °C
3: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / 10 h / -78 - 20 °C
With
1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; iodine; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1016/j.tetlet.2012.02.090
