(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

Base Information

Chemical Name:(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis
CAS No.:116729-99-8
Molecular Formula:C₂₆H₄₁N₃O₈S₂
Molecular Weight:587.759
Hs Code.:

(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis<p-toluenesulfonamide>

Synonyms:(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

Suppliers and Price of (R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

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Technology Process of (R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

There total 7 articles about (R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 116729-87-4
(R)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

: 116729-99-8
(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

Guidance literature:: With Rh/Al₂O₃; hydrogen; In acetic acid; for 48h; Ambient temperature;
DOI:10.1002/hlca.19880710402

Reference yield: 60.0%

: 116729-97-6
(R,R)-4-(methoxymethoxy)-N-<4-(methoxymethoxy)-3-<(p-toluenesulfonyl)amino>butyl>-3-<(p-toluenesulfonyl)amino>butanamide

: 116729-99-8
(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 60 ℃; for 24h;
DOI:10.1002/hlca.19880710402

Reference yield:

: 116729-85-2
(R)-N-(1-cyano-3-hydroxypropan-2-yl)-p-toluenesulfonamide

: 116729-99-8
(R,R)-N,N'-<4,4'-iminobis<1-(methoxymethoxy)butan-2-yl>>bis

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / P₂O₅, molecular sieves / CH₂Cl₂ / 120 h / Ambient temperature

2: 75 percent / CoCl₂, NaBH₄ / methanol / 0.75 h / Ambient temperature

3: 1.) 1,1'-carbonyldiimidazole / 1.) CH₂Cl₂, 1 h; 2.) CH₂Cl₂, r.t., 24 h

4: 60 percent / LiAlH₄ / tetrahydrofuran / 24 h / 60 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; molecular sieve; phosphorus pentoxide; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.19880710402