[2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

Base Information

Chemical Name:[2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester
CAS No.:1402229-01-9
Molecular Formula:C₂₁H₂₅N₇OS₂
Molecular Weight:455.608
Hs Code.:

Synonyms:[2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

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Chemical Property of [2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

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Technology Process of [2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

There total 2 articles about [2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1402228-85-6
3-amino-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-3-piperidin-1-yl-acrylonitrile

: 77-78-1
dimethyl sulfate

: 1402229-01-9
[2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

Guidance literature:: 3-amino-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-3-piperidin-1-yl-acrylonitrile; With carbon disulfide; sodium hydroxide; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

dimethyl sulfate; In water; N,N-dimethyl-formamide; at 5 - 10 ℃; for 3h;
DOI:10.1002/jhet.855

Reference yield:

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 1402229-01-9
[2-cyano-2-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-ylazo)-1-piperidin-1-yl-vinyl]-dithiocarbamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate / ethanol

2.1: ethanol / 5 h / 90 °C

3.1: carbon disulfide; sodium hydroxide / N,N-dimethyl-formamide; water / 0.5 h / 20 °C

3.2: 3 h / 5 - 10 °C

With carbon disulfide; sodium acetate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.855