Technology Process of C14H12BrF4NO2
There total 8 articles about C14H12BrF4NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C14H13BrF3NO3;
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
at 20 ℃;
for 1h;
With
sodium hydrogencarbonate;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / 1,4-dioxane; water / 0.5 h / 20 °C
2.1: sodium hydroxide / water; tetrahydrofuran / 15 °C / pH 10 - 11
2.2: pH 2
3.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 8 °C
4.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 2 h / 20 °C
5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 20 °C
With
hydrogenchloride; diethylamino-sulfur trifluoride; sodium hydrogencarbonate; tetrabutylammonium triphenyldifluorosilicate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water; tetrahydrofuran / 15 °C / pH 10 - 11
1.2: pH 2
2.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 8 °C
3.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 2 h / 20 °C
4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 20 °C
With
diethylamino-sulfur trifluoride; sodium hydrogencarbonate; tetrabutylammonium triphenyldifluorosilicate; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;