ReClN₂(C₆H₅P(OCH₃)2)4

Base Information

Chemical Name:ReClN₂(C₆H₅P(OCH₃)2)4
CAS No.:124608-08-8
Molecular Formula:C₃₂H₄₄ClN₂O₈P₄Re
Molecular Weight:930.265
Hs Code.:

ReClN<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>P(OCH<sub>3</sub>)2)4

Synonyms:ReClN₂(C₆H₅P(OCH₃)2)4

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Chemical Property of ReClN₂(C₆H₅P(OCH₃)2)4

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Technology Process of ReClN₂(C₆H₅P(OCH₃)2)4

There total 2 articles about ReClN₂(C₆H₅P(OCH₃)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2946-61-4
phenylphosphonous acid dimethyl ester

: rhenum(V) dichloro-η2-benzoylhydrazido(3-) bis(triphenylphosphine)

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 124608-08-8
chloro(dinitrogen)(PhP(OMe)2)4rhenium

: 603-35-0
triphenylphosphine

Guidance literature:: With methanol; In methanol; benzene; byproducts: HCl; addn. of PPh(OMe)2 to the Re compd. in benzene under inert gas flow, refluxing for 5 min, concn. (vac.), addn. of MeOH, heating and concn. at elevated temp.; addn. of Et2O, filtn., washing with Et2O, drying in vac. and recrystn. from THF-Et2O; elem. anal.;

Reference yield:

: 2946-61-4
phenylphosphonous acid dimethyl ester

: rhenum(V) dichloro-η2-benzoylhydrazido(3-) bis(triphenylphosphine)

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 124608-08-8
ReClN₂(C₆H₅P(OCH₃)2)4

Guidance literature:: With methanol; In benzene; byproducts: HCl, PPh3; refluxing, then addn. of hot MeOH;
DOI:10.1016/S0277-5387(00)80640-3

Reference yield: 40.0%

: 593-75-9,685498-28-6
methyl isocyanate

: 124608-08-8
chloro(dinitrogen)(PhP(OMe)2)4rhenium

: 2946-61-4
phenylphosphonous acid dimethyl ester

: chloro(methylisocyanide)3(P(OMe)3)2rhenium*0.75CH₂Cl₂

Guidance literature:: In tetrahydrofuran; byproducts: N2; addn. of the isocyanide to the Re compd. in THF and stirring for 2 h at room temp.; filtn., concn. (vac.), addn. of CH2Cl2 or THF followed by Et2O, filtn., washing with Et2O and drying in vac.; elem. anal.;