tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

Base Information

Chemical Name:tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester
CAS No.:84983-67-5
Molecular Formula:C₂₆H₄₀N₄O₉
Molecular Weight:552.625
Hs Code.:

tert.-butyloxycarbonylalanyl-N<sup>ε</sup>-benzyloxycarbonyllysyl-serine methyl ester

Synonyms:tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

There total 5 articles about tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 17693-17-3
N-(tert-butoxycarbonyl)-L-alanine pentachlorophenyl ester

: 110523-34-7
N^ε-benzyloxycarbonyllysyl-serine methyl ester hydrochloride

: 84983-67-5
tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

Guidance literature:: With 1-ethyl-piperidine; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

Reference yield:

: 16948-04-2,76477-42-4
N^α-tert-butyloxycarbonyl-N^ε-benzyloxycarbonyllysine dicyclohexylammonium salt

: 84983-67-5
tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HOBT, WSCl, NMM / tetrahydrofuran / 16 h / 4 °C

2: 1.) TFA, anisole 2.) HOBT, WSCl, NMM / 1.) room temperature, 20 min 2.) DMF, 4 deg C, overnight

With 4-methyl-morpholine; benzotriazol-1-ol; methoxybenzene; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1248/cpb.30.4448

Reference yield:

: N^α-2-nitrobenzenesulfenyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

: 84983-67-5
tert.-butyloxycarbonylalanyl-N^ε-benzyloxycarbonyllysyl-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HCl / acetic acid; methanol / 0.75 h / Ambient temperature

2: 91 percent / N-ethylpiperidine / dimethylformamide / 12 h / Ambient temperature

With 1-ethyl-piperidine; hydrogenchloride; In methanol; acetic acid; N,N-dimethyl-formamide;