C₄₁H₆₈O₁₀Si₂

Base Information

Chemical Name:C₄₁H₆₈O₁₀Si₂
CAS No.:153145-42-7
Molecular Formula:C₄₁H₆₈O₁₀Si₂
Molecular Weight:777.156
Hs Code.:

C<sub>41</sub>H<sub>68</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₁H₆₈O₁₀Si₂

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Chemical Property of C₄₁H₆₈O₁₀Si₂

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Technology Process of C₄₁H₆₈O₁₀Si₂

There total 12 articles about C₄₁H₆₈O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 153145-39-2
C₄₁H₆₆O₈Si₂

: 153145-42-7
C₄₁H₆₈O₁₀Si₂

Guidance literature:: With pyridine; osmium(VIII) oxide; In diethyl ether; at 0 ℃; for 12h;

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-42-7
C₄₁H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

With pyridine; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-42-7
C₄₁H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

With pyridine; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;