C₂₉H₃₃BrN₂O₃

Base Information

Chemical Name:C₂₉H₃₃BrN₂O₃
CAS No.:1447766-90-6
Molecular Formula:C₂₉H₃₃BrN₂O₃
Molecular Weight:537.497
Hs Code.:

C<sub>29</sub>H<sub>33</sub>BrN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₉H₃₃BrN₂O₃

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Chemical Property of C₂₉H₃₃BrN₂O₃

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Technology Process of C₂₉H₃₃BrN₂O₃

There total 3 articles about C₂₉H₃₃BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1447766-82-6
C₂₈H₃₁BrN₂O₃

: 1774-47-6
trimethylsulfoxonium iodide

: 1447766-90-6
C₂₉H₃₃BrN₂O₃

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; mineral oil; for 0.75h; Inert atmosphere;

C₂₈H₃₁BrN₂O₃; In tetrahydrofuran; dimethyl sulfoxide; mineral oil; at 20 ℃; for 30h; Inert atmosphere;
DOI:10.1021/ja405548b

Reference yield:

: C₂₂H₂₂BrNO₂

: 1447766-90-6
C₂₉H₃₃BrN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: 2.5 h / -78 - 20 °C / Inert atmosphere

2.1: L-proline / dichloromethane; acetonitrile / 216 h / Inert atmosphere

3.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

3.2: 30 h / 20 °C / Inert atmosphere

With oxalyl dichloride; sodium hydride; dimethyl sulfoxide; L-proline; In dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil; 1.1: |Swern Oxidation;
DOI:10.1021/ja405548b

Reference yield:

: 1447766-83-7
C₂₂H₂₀BrNO₂

: 1447766-90-6
C₂₉H₃₃BrN₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: L-proline / dichloromethane; acetonitrile / 216 h / Inert atmosphere

2.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / Inert atmosphere

2.2: 30 h / 20 °C / Inert atmosphere

With sodium hydride; L-proline; In dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ja405548b