1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane

Base Information

• Chemical Name: 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane
• CAS No.: 871123-19-2
• Molecular Formula: C₃₄H₂₇NO₆
• Molecular Weight: 545.591
• Mol file: 871123-19-2.mol

Synonyms:1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane

Chemical Property of 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane

There total 3 articles about 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(4-aminophenyl)-1,1-bis(4-(4'-cyanophenoxy)phenyl)ethane (871123-18-1) → 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane (871123-19-2)

Guidance literature:

With potassium hydroxide; In ethanol; water; for 12h; Heating;

DOI:10.1021/ma051538y

Reference yield:

4-fluorobenzonitrile (1194-02-1,143234-87-1) → 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane (871123-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / K₂CO₃ / benzene; N,N-dimethyl-acetamide / 4 h / 100 - 120 °C

2: 95 percent / KOH / ethanol; H₂O / 12 h / Heating

With potassium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl acetamide; water; benzene;

DOI:10.1021/ma051538y

Reference yield:

1-(4-aminophenyl)-1,1-bis(4-hydroxyphenyl)ethane (266001-57-4) → 1-(4-aminophenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane (871123-19-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / K₂CO₃ / benzene; N,N-dimethyl-acetamide / 4 h / 100 - 120 °C

2: 95 percent / KOH / ethanol; H₂O / 12 h / Heating

With potassium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl acetamide; water; benzene;

DOI:10.1021/ma051538y

upstream raw materials:

1-(4-aminophenyl)-1,1-bis(4-(4'-cyanophenoxy)phenyl)ethane

4-fluorobenzonitrile

1-(4-aminophenyl)-1,1-bis(4-hydroxyphenyl)ethane

Downstream raw materials:

1-(4-(4'-fluorobenzamido)phenyl)-1,1-bis(4-(4'-carboxyphenoxy)phenyl)ethane

CCH₃(C₆H₄OC₆H₄COCl)2C₆H₄NHCOC₆H₄F