C₆₂H₁₁₁NO₁₀SeSi₄

Base Information

Chemical Name:C₆₂H₁₁₁NO₁₀SeSi₄
CAS No.:1033588-19-0
Molecular Formula:C₆₂H₁₁₁NO₁₀SeSi₄
Molecular Weight:1221.87
Hs Code.:

C<sub>62</sub>H<sub>111</sub>NO<sub>10</sub>SeSi<sub>4</sub>

Synonyms:C₆₂H₁₁₁NO₁₀SeSi₄

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Chemical Property of C₆₂H₁₁₁NO₁₀SeSi₄

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Technology Process of C₆₂H₁₁₁NO₁₀SeSi₄

There total 36 articles about C₆₂H₁₁₁NO₁₀SeSi₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 1033588-17-8
C₅₆H₁₀₈O₉Si₄

: 1033588-19-0
C₆₂H₁₁₁NO₁₀SeSi₄

Guidance literature:: With tributylphosphine; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1021/ja803012n

Reference yield:

: C₂₉H₄₈O₅Si

: 1033588-19-0
C₆₂H₁₁₁NO₁₀SeSi₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - -40 °C / Inert atmosphere

2.3: 0.5 h / -40 °C / Inert atmosphere

3.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: water; acetic acid / tetrahydrofuran / 5 h / -20 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 12 h / 20 °C / Inert atmosphere

5.2: 19 h / 20 °C / Inert atmosphere

6.1: methanol; barium hydroxide octahydrate / 0.33 h / 20 °C

7.1: tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C

7.2: 24 h / 20 °C

8.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran; dichloromethane; toluene / 0.75 h / -20 °C / Inert atmosphere

9.1: titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 5 h / -20 °C / Molecular sieve; Inert atmosphere

10.1: tributylphosphine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; dmap; sodium periodate; tetrapropylammonium perruthennate; barium hydroxide octahydrate; tributylphosphine; dimethylsulfide borane complex; 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; decane; dichloromethane; toluene; 9.1: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo3026077

Reference yield:

: 1033588-06-5
C₂₂H₄₀O₄Si

: 1033588-19-0
C₆₂H₁₁₁NO₁₀SeSi₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

1.2: -78 - -40 °C / Inert atmosphere

1.3: 0.5 h / -40 °C / Inert atmosphere

2.1: dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 5 h / -20 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 12 h / 20 °C / Inert atmosphere

4.2: 19 h / 20 °C / Inert atmosphere

5.1: methanol; barium hydroxide octahydrate / 0.33 h / 20 °C

6.1: tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C

6.2: 24 h / 20 °C

7.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran; dichloromethane; toluene / 0.75 h / -20 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 5 h / -20 °C / Molecular sieve; Inert atmosphere

9.1: tributylphosphine / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; dmap; tetrapropylammonium perruthennate; barium hydroxide octahydrate; tributylphosphine; dimethylsulfide borane complex; 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; In tetrahydrofuran; decane; dichloromethane; toluene; 8.1: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo3026077