Technology Process of C66H85BrN4O8SiZn
There total 8 articles about C66H85BrN4O8SiZn which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; triphenylphosphine;
In
triethylamine; toluene;
(N2); drying mixt. of porphyrin deriv., palladium compd., phosphine deriv. and CuI at 40°C for 4 h, addn. of toluene and triethylamine under N2, degassing, addn. of acetylene deriv. at room temp., stirring at 40°C for 3 h; addn. of CH2Cl2, filtration through silica eluting with 97:3 CH2Cl2/methanol, chromy. (silica, CH2Cl2/methanol (199:1)), size exclusion chromy. (Bio Beads S-X1, THF), evapn., NMR and MALDI;
DOI:10.1039/b814789b
- Guidance literature:
-
With
triethylamine; triphenylphosphine;
tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide;
In
toluene;
at 20 - 40 ℃;
for 3h;
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; triethylamine; triphenylphosphine;
In
toluene;
at 20 - 40 ℃;
Inert atmosphere;
DOI:10.1039/b814789b
