Technology Process of C13H17IO
There total 4 articles about C13H17IO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole; iodine; triphenylphosphine;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1021/jo2002616
- Guidance literature:
-
Multi-step reaction with 4 steps
1: titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -40 - -30 °C / Molecular sieve
2: trifluorormethanesulfonic acid / diethyl ether / 0 - 20 °C
3: lithium borohydride / tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere
4: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With
1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium borohydride; trifluorormethanesulfonic acid; iodine; D-(-)-diisopropyl tartrate; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane;
1: Sharpless epoxidation;
DOI:10.1021/jo2002616
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluorormethanesulfonic acid / diethyl ether / 0 - 20 °C
2: lithium borohydride / tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere
3: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With
1H-imidazole; lithium borohydride; trifluorormethanesulfonic acid; iodine; triphenylphosphine;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jo2002616
