13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

Base Information

Chemical Name:13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one
CAS No.:884850-58-2
Molecular Formula:C₃₅H₃₁N₃O₅
Molecular Weight:573.648
Hs Code.:

13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13<i>H</i>-8,10-dioxa-6,13-diaza-cyclopenta[<i>b</i>]chrysen-12-one

Synonyms:13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

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Chemical Property of 13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

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Technology Process of 13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

There total 10 articles about 13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 884850-52-6
6,7-methylenedioxyquinoline-4-carboxylic acid N-[2-(N,N-dibenzylamino)ethyl]-N-(2-iodo-4,5-dimethoxyphenyl)amide

: 884850-58-2
13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

Guidance literature:: With silver carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 2h; Heating;
DOI:10.1016/j.bmc.2005.12.028

Reference yield:

: 881-70-9
3',4'-dimethoxyacetanilide

: 884850-58-2
13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / iodine monochloride; acetic acid / CH₂Cl₂

2: 93 percent / NaOH / ethanol; H₂O / 4 h / Heating

3: 512 mg / triethylamine / CH₂Cl₂ / Heating

4: 85 percent / sodium hydride; sodium iodide / dimethylformamide; various solvent(s) / 6 h / 60 °C

5: 23 percent / Ag₂CO₃ / Pd(PPh₃)4 / dimethylformamide / 2 h / Heating

With sodium hydroxide; Iodine monochloride; sodium hydride; acetic acid; triethylamine; silver carbonate; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; 5: Heck cyclization;
DOI:10.1016/j.bmc.2005.12.028

Reference yield:

: 14268-66-7
benzo[1,3]dioxolo-5-ylamine

: 884850-58-2
13-(2-dibenzylamino-ethyl)-2,3-dimethoxy-13H-8,10-dioxa-6,13-diaza-cyclopenta[b]chrysen-12-one

Guidance literature:: Multi-step reaction with 7 steps

1: 44 percent / iron(III) chloride; acetic acid / 1.5 h / Heating

2: 65 percent / SeO₂ / dioxane; H₂O / 4.5 h / Heating

3: 90 percent / potassium permanganate; pyridine / H₂O / -5 - 20 °C

4: thionyl chloride / 2 h / Heating

5: 512 mg / triethylamine / CH₂Cl₂ / Heating

6: 85 percent / sodium hydride; sodium iodide / dimethylformamide; various solvent(s) / 6 h / 60 °C

7: 23 percent / Ag₂CO₃ / Pd(PPh₃)4 / dimethylformamide / 2 h / Heating

With pyridine; potassium permanganate; selenium(IV) oxide; thionyl chloride; iron(III) chloride; sodium hydride; acetic acid; triethylamine; silver carbonate; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 7: Heck cyclization;
DOI:10.1016/j.bmc.2005.12.028