methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

Base Information

Chemical Name:methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside
CAS No.:1607435-09-5
Molecular Formula:C₂₂H₃₅N₃O₄S
Molecular Weight:437.604
Hs Code.:

Synonyms:methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

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Chemical Property of methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

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Technology Process of methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

There total 6 articles about methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1607435-28-8
C₁₅H₃₀N₂O₄

: 103-72-0
phenyl isothiocyanate

: 1607435-09-5
methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: In methanol; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2013.12.026

Reference yield:

: 56543-17-0
methyl 4-O-benzoyl-6-bromo-6-deoxy-2,3-di-O-methyl-α-D-glucopyranoside

: 1607435-09-5
methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide / N,N-dimethyl-formamide / 6 h / 70 °C

2: sodium methylate / methanol / 1 h / 20 °C

3: trifluoromethylsulfonic anhydride / dichloromethane; pyridine / 2 h / 0 °C

4: N,N-dimethyl-formamide / 10 h / 45 °C

5: 1.3-propanedithiol / methanol / 48 h / 20 °C

6: methanol / 4 h / 20 °C

With 1.3-propanedithiol; sodium azide; trifluoromethylsulfonic anhydride; sodium methylate; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2013.12.026

Reference yield:

: 1607435-07-3
methyl 6-azido-4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-α-D-galactopyranoside

: 1607435-09-5
methyl 4-cyclohexylamino-4,6-dideoxy-2,3-di-O-methyl-6-(N'-phenyl)thioureido-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.3-propanedithiol / methanol / 48 h / 20 °C

2: methanol / 4 h / 20 °C

With 1.3-propanedithiol; In methanol;
DOI:10.1016/j.carres.2013.12.026