2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Base Information

Chemical Name:2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide
CAS No.:1562665-26-2
Molecular Formula:C₂₃H₁₉ClN₄O₅S₂
Molecular Weight:531.013
Hs Code.:

Synonyms:2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Suppliers and Price of 2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

There total 5 articles about 2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 10147-70-3
2-chloro-N-(2-nitrophenyl)acetamide

: 1221883-92-6
6-chloro-1-(3,5-dimethylphenylsulfonyl)-1,3-dihydro-2H-benzimidazole-2-thione

: 1562665-26-2
2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2013.12.045

Reference yield:

: 934417-63-7
N-(2-amino-5-chlorophenyl)-3,5-dimethylbenzenesulfonamide

: 1562665-26-2
2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With potassium carbonate; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.12.045

Reference yield:

: 934417-61-5
N-(5-chloro-2-nitrophenyl)-3,5-dimethylbenzenesulfonamide

: 1562665-26-2
2-({6-chloro-1-[(3,5-dimethylphenyl)sulfonyl]-1H-benzimidazol-2-yl}sulfanyl)-N-2-nitrophenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; zinc / ethanol / 1 h / Reflux

2: pyridine / 1 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With hydrogenchloride; potassium carbonate; zinc; In pyridine; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.12.045