C₄₇H₇₈O₆Si₂

Base Information

Chemical Name:C₄₇H₇₈O₆Si₂
CAS No.:1375412-36-4
Molecular Formula:C₄₇H₇₈O₆Si₂
Molecular Weight:795.304
Hs Code.:

C<sub>47</sub>H<sub>78</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₇H₇₈O₆Si₂

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Chemical Property of C₄₇H₇₈O₆Si₂

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Technology Process of C₄₇H₇₈O₆Si₂

There total 13 articles about C₄₇H₇₈O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1375412-53-5
C₄₄H₇₃IO₆Si₂

: 24850-33-7
allyltributylstanane

: 1375412-36-4
C₄₇H₇₈O₆Si₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane; In N,N-dimethyl-formamide; for 1.5h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-36-4
C₄₇H₇₈O₆Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: dilithium tetrachlorocuprate / tetrahydrofuran / 1.5 h / 0 °C

3.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

5.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

6.2: 1 h / -50 - -45 °C

6.3: 2 h / -70 - 0 °C

7.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

8.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

9.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

10.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-Bromosuccinimide; (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; samarium diiodide; dilithium tetrachlorocuprate; triphenyl-arsane; 2,4,6-trichlorobenzoyl chloride; water; silver perchlorate; sodium hydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; mineral oil; 4.1: Corey-Chaykovsky reaction / 5.1: Jacobsen hydrolytic kinetic resolution / 6.3: Brook rearrangement / 8.1: Evans-Tishchenko reduction / 10.1: Stille coupling;
DOI:10.1002/anie.201108692

Reference yield:

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

: 1375412-36-4
C₄₇H₇₈O₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

2: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

3: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

4: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; samarium diiodide; triphenyl-arsane; 2,4,6-trichlorobenzoyl chloride; silver perchlorate; dihydropyrimidinone; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; toluene; 2: Evans-Tishchenko reduction / 4: Stille coupling;
DOI:10.1002/anie.201108692