1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

Base Information

Chemical Name:1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide
CAS No.:132816-31-0
Molecular Formula:C₃₁H₄₄N₂O₁₁
Molecular Weight:620.697
Hs Code.:

1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

Synonyms:1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

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Chemical Property of 1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

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Technology Process of 1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

There total 2 articles about 1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 78699-90-8
N-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethyl)-hydroxylamine

: 132816-30-9
1-deoxy-1-(4-fromylbenzylidenamino)-2,3:4,5-di-O-ispropylidene-α-D-arabinitol N-oxide

: 132816-31-0
1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

Guidance literature:: With pyridine; In ethanol; for 12h; Ambient temperature;
DOI:10.1016/0008-6215(91)80167-L

Reference yield:

: 623-27-8
terephthalaldehyde,

: 132816-31-0
1-(6-deoxy-1,2:3,4-di-O-ispropylidene-α-D-galactopyranos-6-yliminomethyl)-4-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-arabinitol-1-yliminomethyl)benzene bis-N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / pyridine / ethanol / 12 h / Ambient temperature

2: 89 percent / pyridine / ethanol / 12 h / Ambient temperature

With pyridine; In ethanol;
DOI:10.1016/0008-6215(91)80167-L