(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

Base Information

Chemical Name:(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine
CAS No.:862563-54-0
Molecular Formula:C₁₉H₂₃NO₃S
Molecular Weight:345.463
Hs Code.:

Synonyms:(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

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Chemical Property of (2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

Chemical Property:

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Technology Process of (2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

There total 9 articles about (2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [1-((S)-2-Benzenesulfonyl-1-methyl-cyclohex-2-enyl)-meth-(E)-ylidene]-furan-2-ylmethyl-amine

: 862563-54-0
(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h;
DOI:10.1021/ol051184v

Reference yield:

: 172825-16-0
(1R)-1-methyl-2-oxo-cyclohexanecarboxylic acid ethyl ester

: 862563-54-0
(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

Guidance literature:: Multi-step reaction with 6 steps

1: P₂O₅ / CH₂Cl₂ / 48 h / 23 °C

2: DIBAL-H / toluene; hexane / 0.33 h / 0 °C

3: 0.188 g / IBX / dimethylsulfoxide / 4 h / 23 °C

4: 94 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

5: Et₃N; molecular sieves 3 Angstroem / methanol / 12 h / 23 °C

6: 0.38 g / NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; 3 A molecular sieve; phosphorus pentoxide; diisobutylaluminium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/ol051184v

Reference yield:

: 862563-52-8
1-methyl-2-phenylsulfanyl-cyclohex-2-enecarbaldehyde

: 862563-54-0
(2-benzenesulfonyl-1-methyl-cyclohex-2-enylmethyl)-furan-2-ylmethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / mCPBA / CH₂Cl₂ / 1 h / 0 °C

2: Et₃N; molecular sieves 3 Angstroem / methanol / 12 h / 23 °C

3: 0.38 g / NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; 3 A molecular sieve; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1021/ol051184v