Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-

Base Information

Chemical Name:Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-
CAS No.:227766-19-0
Molecular Formula:C₁₀H₂₁NO₂S
Molecular Weight:219.348
Hs Code.:
Mol file:227766-19-0.mol

Synonyms:Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-

Suppliers and Price of Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl-

There total 4 articles about Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S-(1,1-dimethylethyl)-S-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6163-64-0
tert-butyl methyl sulphide

: 462100-44-3
oxaziridine-2,3,3-tricarboxylic acid 2-tert-butyl ester 3,3-diethyl ester

: 227766-19-0
tert-butyl N-tert-butyloxycarbonyl methyl sulfimine

Guidance literature:: In dichloromethane; at -40 - 20 ℃; for 0.5h;
DOI:10.1039/b201791a

Reference yield: 6.0%

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 6163-64-0
tert-butyl methyl sulphide

: 227766-19-0
tert-butyl N-tert-butyloxycarbonyl methyl sulfimine

Guidance literature:: iron(II) chloride; In dichloromethane; Ambient temperature;
DOI:10.1002/(SICI)1099-0690(199905)1999:5<1033::AID-EJOC1033>3.0.CO;2-1

Reference yield:

: 68014-21-1
triphenyl(t-butoxycarbonylimino)phosphorane

: 227766-19-0
tert-butyl N-tert-butyloxycarbonyl methyl sulfimine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 18 h / Heating

2: 7.68 g / mCPBA; BuLi / CH₂Cl₂ / 2 h / -78 °C

3: 75 percent / CH₂Cl₂ / 0.5 h / -40 - 20 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b201791a