5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

Base Information

Chemical Name:5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide
CAS No.:1034354-86-3
Molecular Formula:C₂₀H₂₀ClFN₂O₂S
Molecular Weight:406.908
Hs Code.:

Synonyms:5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

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Chemical Property of 5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

Chemical Property:

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Technology Process of 5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

There total 3 articles about 5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 446-48-0
o-fluorobenzyl bromide

: 1034835-84-1
Z-5-chloro-N-(5,5-dimethyl-4,5-dihydrothiazol-2-yl)-2-methoxybenzamide

: 1034354-86-3
5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

Guidance literature:: With C₁₃H₃₀N₄PPol; In N,N-dimethyl acetamide; at 70 ℃;

Reference yield:

: 3438-16-2
5-chloro-2-methoxybenzoic acid

: 1034354-86-3
5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 1 h / 20 °C

2: C₁₃H₃₀N₄PPol / N,N-dimethyl acetamide / 70 °C

With C₁₃H₃₀N₄PPol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; N,N-dimethyl acetamide;

Reference yield:

: 21018-37-1
5,5-dimethyl-4,5-dihydro-thiazol-2-ylamine; hydrochloride

: 1034354-86-3
5-chloro-N-[(2Z)-3-(2-fluorobenzyl)-5,5-dimethyl-1,3-thiazolidin-2-ylidene]-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 1 h / 20 °C

2: C₁₃H₃₀N₄PPol / N,N-dimethyl acetamide / 70 °C

With C₁₃H₃₀N₄PPol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; N,N-dimethyl acetamide;