(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

Base Information

Chemical Name:(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate
CAS No.:1426855-37-9
Molecular Formula:C₁₃H₁₇Br₂NO₄
Molecular Weight:411.09
Hs Code.:

Synonyms:(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

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Chemical Property of (±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

Chemical Property:

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Technology Process of (±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

There total 3 articles about (±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 104-14-3,1915-83-9
octopamine

: 24424-99-5
di-tert-butyl dicarbonate

: 1426855-37-9
(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

Guidance literature:: octopamine; With hydrogenchloride; bromine; In water; at 5 - 20 ℃; for 1h;

di-tert-butyl dicarbonate; With sodium hydroxide; at 20 ℃; for 0.5h;
DOI:10.1021/np300648d

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 80573-77-9
C₈H₉Br₂NO₂

: 1426855-37-9
(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201500603

Reference yield:

: 104-14-3,1915-83-9
octopamine

: 1426855-37-9
(±)-tert-butyl 2-(3,5-dibromo-4-hydroxyphenyl)-2-hydroxyethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; hydrogenchloride / water / 1 h / 5 °C / Inert atmosphere

2: sodium hydroxide / water / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; bromine; sodium hydroxide; In water;
DOI:10.1002/ejoc.201500603