1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Base Information

Chemical Name:1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate
CAS No.:1239349-15-5
Molecular Formula:C₅₂H₄₉BrN₆O₆
Molecular Weight:933.902
Hs Code.:

Synonyms:1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Suppliers and Price of 1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

There total 2 articles about 1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1239349-14-4
2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)bi-phenyl-4-yl)methylamino)methyleneamino)benzoic acid

: 99464-83-2
1-chloroethyl cyclohexyl carbonate

: 1239349-15-5
1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Guidance literature:: 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)bi-phenyl-4-yl)methylamino)methyleneamino)benzoic acid; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃;

1-chloroethyl cyclohexyl carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 8h;
DOI:10.1016/j.tet.2010.05.037

Reference yield: 70.0%

: 1239349-13-3
methyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

: 99464-83-2
1-chloroethyl cyclohexyl carbonate

: 1239349-15-5
1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

Guidance literature:: methyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

1-chloroethyl cyclohexyl carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 8h;
DOI:10.1016/j.tet.2010.05.037

Reference yield: 75.0%

: 1239349-15-5
1-(cyclohexyloxycarbonyloxy)ethyl 2-bromo-3-(ethoxy(1-(2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl)methylamino)methyleneamino)benzoate

: 170791-09-0
cilexetil trityl candesartan

Guidance literature:: With copper(l) iodide; potassium carbonate; L-proline; In dimethyl sulfoxide; at 70 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.037