Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI)

Base Information

Chemical Name:Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI)
CAS No.:227766-17-8
Molecular Formula:C₇H₁₅NO₂S
Molecular Weight:177.268
Hs Code.:
Mol file:227766-17-8.mol

Synonyms:Sulfilimine,N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI)

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Chemical Property of Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI)

Chemical Property:

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Technology Process of Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI)

There total 4 articles about Sulfilimine, N-[(1,1-dimethylethoxy)carbonyl]-S,S-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 75-18-3
dimethylsulfide

: 462100-44-3
oxaziridine-2,3,3-tricarboxylic acid 2-tert-butyl ester 3,3-diethyl ester

: 227766-17-8
N-tert-butyloxycarbonyl dimethyl sulfimine

Guidance literature:: In dichloromethane; at -40 - 20 ℃; for 0.5h;
DOI:10.1039/b201791a

Reference yield: 27.0%

: 1070-19-5
N-(tert-butyloxycarbonyl) azide

: 75-18-3
dimethylsulfide

: 227766-17-8
N-tert-butyloxycarbonyl dimethyl sulfimine

Guidance literature:: iron(II) chloride; In dichloromethane; Ambient temperature;
DOI:10.1002/(SICI)1099-0690(199905)1999:5<1033::AID-EJOC1033>3.0.CO;2-1

Reference yield:

: 68014-21-1
triphenyl(t-butoxycarbonylimino)phosphorane

: 227766-17-8
N-tert-butyloxycarbonyl dimethyl sulfimine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 18 h / Heating

2: 7.68 g / mCPBA; BuLi / CH₂Cl₂ / 2 h / -78 °C

3: 49 percent / CH₂Cl₂ / 0.5 h / -40 - 20 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b201791a