(+)-8'-epihydroxythujaplicatin methyl ether

Base Information

Chemical Name:(+)-8'-epihydroxythujaplicatin methyl ether
CAS No.:135095-51-1
Molecular Formula:C₂₁H₂₄O₈
Molecular Weight:404.417
Hs Code.:

Synonyms:(+)-8'-epihydroxythujaplicatin methyl ether

Suppliers and Price of (+)-8'-epihydroxythujaplicatin methyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-8'-epihydroxythujaplicatin methyl ether

Chemical Property:

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Technology Process of (+)-8'-epihydroxythujaplicatin methyl ether

There total 2 articles about (+)-8'-epihydroxythujaplicatin methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 135095-50-0
(-)-O-dibenzyl-8'-epihydroxythujaplicatin methyl ether

: 135095-51-1
(+)-8'-epihydroxythujaplicatin methyl ether

Guidance literature:: With hydrogen; Pd-Pt/C; In ethanol; ethyl acetate; for 16h; under 2250.2 Torr; Ambient temperature;

Reference yield:

: 111194-06-0
(-)-O-dibenzylthujaplicatin methyl ether

: 135095-51-1
(+)-8'-epihydroxythujaplicatin methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium hexamethyldisilazide (LHDS), 2.) O₂, 12-crown-4, triethyl phosphite / 1.) benzene, RT, 2 h, 2.) 3 h

2: 73 percent / H₂ / 10percent Pd-Pt/C / ethanol; ethyl acetate / 16 h / 2250.2 Torr / Ambient temperature

With (1,4,7,10-tetraoxacyclododecane); hydrogen; oxygen; lithium hexamethyldisilazane; triethyl phosphite; Pd-Pt/C; In ethanol; ethyl acetate;