9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

Base Information

Chemical Name:9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene
CAS No.:106933-06-6
Molecular Formula:C₂₀H₂₉Cl
Molecular Weight:304.903
Hs Code.:

Synonyms:9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

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Chemical Property of 9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

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Technology Process of 9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

There total 2 articles about 9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 103200-77-7
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-nonadien-14-yn-13-ol

: 106933-06-6
9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

Guidance literature:: With hydrogenchloride; In acetone; at 20 - 25 ℃; for 0.0833333h;

Reference yield:

: 51077-54-4
9,13-dimethyl-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-9,11-heptadien-13-one

: 106933-06-6
9,13-dimethyl-14-chloro-7-(1,1,5-trimethyl-5-cyclohexen-6-yl)-8,10,12,14-nonatetraene

Guidance literature:: Multi-step reaction with 2 steps

1: 63.5 percent / Ca / liquid ammonia; diethyl ether / 3 h / -45 - -40 °C

2: 43 percent / conc. aq. HCl / acetone / 0.08 h / 20 - 25 °C

With hydrogenchloride; calcium; In diethyl ether; ammonia; acetone;