methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

Base Information

Chemical Name:methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate
CAS No.:1352622-01-5
Molecular Formula:C₁₇H₁₅BrCl₃NO₅S
Molecular Weight:531.639
Hs Code.:

Synonyms:methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

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Chemical Property of methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

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Technology Process of methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

There total 4 articles about methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1352621-86-3
2,4,6-trichlorophenyl 1-bromoethenesulfonate

: 18358-63-9
methyl 4-(N-methyl)aminobenzoate

: 1352622-01-5
methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

Guidance literature:: at 130 ℃; for 2h; Neat (no solvent);
DOI:10.1016/j.tetlet.2011.10.093

Reference yield:

: 4790-35-6
ethenesulfonic acid 2,4,6-trichlorophenyl ester

: 1352622-01-5
methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2'-azobis(isobutyronitrile); bromine / 1,2-dichloro-ethane / 3 h / Reflux

1.2: 1.08 h / -78 - 20 °C

2.1: 2 h / 130 °C / Neat (no solvent)

With 2,2'-azobis(isobutyronitrile); bromine; In 1,2-dichloro-ethane; 2.1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093

Reference yield:

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 1352622-01-5
methyl 4-((2-bromo-2-((2,4,6-trichlorophenoxy)sulfonyl)ethyl)(methyl)amino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / -78 - 20 °C

2.1: 2,2'-azobis(isobutyronitrile); bromine / 1,2-dichloro-ethane / 3 h / Reflux

2.2: 1.08 h / -78 - 20 °C

3.1: 2 h / 130 °C / Neat (no solvent)

With 2,2'-azobis(isobutyronitrile); bromine; triethylamine; In dichloromethane; 1,2-dichloro-ethane; 3.1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093