(1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene

Base Information

• Chemical Name: (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene
• CAS No.: 103886-84-6
• Molecular Formula: C₁₉H₁₃ClF₄S
• Molecular Weight: 384.825

Synonyms:(1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene

Chemical Property of (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene

Chemical Property:

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Technology Process of (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene

There total 1 articles about (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylbenzenesulfenyl chloride (933-00-6) + 3,4,5,6-Tetrafluoro-tricyclo[6.2.2.02,7]dodeca-2(7),3,5,9,11-pentaene (5162-34-5) → (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.02,7]dodeca-2(7),3,5,9-tetraene (103886-84-6)

Guidance literature:

In nitromethane; for 0.166667h;

Reference yield: 50.0%

p-methylbenzenesulfenyl chloride (933-00-6) + (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.02,7]dodeca-2(7),3,5,9-tetraene (103886-84-6) → 5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene (103886-83-5)

Guidance literature:

With lithium perchlorate; In nitromethane; at 20 ℃; for 3h;

Reference yield:

p-methylbenzenesulfenyl chloride (933-00-6) + (1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.02,7]dodeca-2(7),3,5,9-tetraene (103886-84-6) → (1S,8R,9R,10R)-9,12-Dichloro-3,4,5,6-tetrafluoro-10,11-bis-p-tolylsulfanyl-tricyclo[6.2.2.02,7]dodeca-2(7),3,5-triene (103886-83-5)

Guidance literature:

With lithium perchlorate; In nitromethane;

upstream raw materials:

p-methylbenzenesulfenyl chloride

3,4,5,6-Tetrafluoro-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9,11-pentaene

Downstream raw materials:

(1S,8R,9R,10R)-9,12-Dichloro-3,4,5,6-tetrafluoro-10,11-bis-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5-triene

5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

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