C₃₅H₅₉Si₂NO₈

Base Information

Chemical Name:C₃₅H₅₉Si₂NO₈
CAS No.:937163-86-5
Molecular Formula:C₃₅H₅₉NO₈Si₂
Molecular Weight:678.026
Hs Code.:

C<sub>35</sub>H<sub>59</sub>Si<sub>2</sub>NO<sub>8</sub>

Synonyms:C₃₅H₅₉Si₂NO₈

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Chemical Property of C₃₅H₅₉Si₂NO₈

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Technology Process of C₃₅H₅₉Si₂NO₈

There total 10 articles about C₃₅H₅₉Si₂NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937163-73-0
C₁₇H₃₄SiO₄

: 937163-86-5
C₃₅H₅₉Si₂NO₈

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

2: 82 percent / NIS / CH₂Cl₂ / 20 °C

3: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

4: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

5: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

6: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

With N-iodo-succinimide; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ol070435s

Reference yield:

: 937164-11-9
C₂₄H₃₈SiO₅

: 937163-86-5
C₃₅H₅₉Si₂NO₈

Guidance literature:: Multi-step reaction with 7 steps

1: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

2: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

3: 82 percent / NIS / CH₂Cl₂ / 20 °C

4: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

5: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

6: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

7: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

With N-iodo-succinimide; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; diisobutylaluminium hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ol070435s

Reference yield:

: 937164-09-5
C₂₂H₃₄SiO₄

: 937163-86-5
C₃₅H₅₉Si₂NO₈

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / P₂O₅ / 0.5 h / 20 °C

2: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

3: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

4: 82 percent / NIS / CH₂Cl₂ / 20 °C

5: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

6: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

7: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

8: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

With N-iodo-succinimide; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; phosphorus pentoxide; diisobutylaluminium hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ol070435s