3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

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Chemical Name:3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester
CAS No.:145487-83-8
Molecular Formula:C₅₅H₇₄N₂O₁₆
Molecular Weight:1019.2
Hs Code.:

3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

Synonyms:3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

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Chemical Property of 3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

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Technology Process of 3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

There total 2 articles about 3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 73554-57-1
6,7-dimethoxy-1-(3',4',5'-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

: 145487-79-2
1,2,14,15-diepoxy-4,12-dioxa-3,13-dioxopentadecane

: 145487-83-8
3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

Guidance literature:: In isopropyl alcohol; at 50 ℃; for 48h;
DOI:10.1016/0223-5234(92)90180-9

Reference yield:

: 61804-12-4
heptane-1,7-diyl diacrylate

: 145487-83-8
3-[6,7-Dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionic acid 7-{3-[6,7-dimethoxy-1-(3,4,5-trimethoxy-benzyl)-3,4-dihydro-1H-isoquinolin-2-yl]-2-hydroxy-propionyloxy}-heptyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85percent H₂O₂, trifluoroacetic anhydride, Na₂HPO₄ / CH₂Cl₂ / 3 h / 42 °C

2: 90 percent / propan-2-ol / 48 h / 50 °C

With disodium hydrogenphosphate; dihydrogen peroxide; trifluoroacetic anhydride; In dichloromethane; isopropyl alcohol;
DOI:10.1016/0223-5234(92)90180-9