2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole
CAS No.:33575-82-5
Molecular Formula:C9H6 Cl2 N2 O
Molecular Weight:229.065
Hs Code.:2934999090
Mol file:33575-82-5.mol

Synonyms:1,3,4-Oxadiazole,2-(chloromethyl)-5-(m-chlorophenyl)- (8CI);2-Chloromethyl-5-(3-chlorophenyl)-1,3,4-oxadiazole

Suppliers and Price of 2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(Chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole
250mg
$ 265.00

American Custom Chemicals Corporation
2-(CHLOROMETHYL)-5-(3-CHLOROPHENYL)-1,3,4-OXADIAZOLE 95.00%
1G
$ 402.15

American Custom Chemicals Corporation
2-(CHLOROMETHYL)-5-(3-CHLOROPHENYL)-1,3,4-OXADIAZOLE 95.00%
2.5G
$ 1147.43

AK Scientific
2-(Chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole
500mg
$ 435.00

Total 2 raw suppliers

Chemical Property of 2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Chemical Property:

PSA：38.92000
LogP:3.12880

Purity/Quality:

98%min ^*data from raw suppliers

2-(Chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

There total 7 articles about 2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 74974-54-2
2-chloro-1,1,1-trimethoxyethane

: 1673-47-8
3-chlorobenzhydrazide

: 33575-82-5
2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Guidance literature:: at 160 ℃; for 0.0833333h; microwave irradiation;
DOI:10.1081/SCC-200025582

Reference yield:

: 63002-49-3
3-Chloro-benzoic acid N'-(2-chloro-acetyl)-hydrazide

: 33575-82-5
2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Guidance literature:: With trichlorophosphate; at 90 - 100 ℃;
DOI:10.1016/j.ejps.2019.104966

Reference yield:

: 535-80-8
3-chlorobenzoate

: 33575-82-5
2-(chloromethyl)-5-(3-chlorophenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; sulfuric acid / methanol

2: trichlorophosphate / 105 - 110 °C

With sulfuric acid; hydrazine hydrate; trichlorophosphate; In methanol;
DOI:10.1016/j.bmcl.2018.04.021