1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

Base Information

Chemical Name:1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose
CAS No.:1092961-86-8
Molecular Formula:C₂₉H₃₈O₈Si
Molecular Weight:542.701
Hs Code.:

Synonyms:1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

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Technology Process of 1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

There total 1 articles about 1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1092961-85-7
(2R,3S,4S)-1-benzoyloxy-2-tert-butyldimethylsilyloxy-5-hydroxy-3,4-O-isopropylidene-hexyl benzoate

: 1092961-86-8
1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2008.09.008

Reference yield:

: 1092961-86-8
1,6-di-O-benzoyl-5-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-D-psicose

: 1,6-di-O-benzoyl-3,4-O-isopropylidene-α-D-psicofuranose

: 1092961-87-9
1,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-psicofuranose

Guidance literature:: With 1H-imidazole; pyridine hydrogenfluoride; In acetonitrile; at 20 ℃; for 24h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetasy.2008.09.008