Technology Process of C28H20N6
There total 4 articles about C28H20N6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 5h;
DOI:10.1039/c3cc48618d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux
2: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
With
N-Bromosuccinimide; sodium azide; dibenzoyl peroxide;
In
tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc48618d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate; water; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 24 h / Inert atmosphere; Reflux
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux
3: sodium azide / N,N-dimethyl-formamide / 5 h / 50 °C
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sodium azide; water; sodium carbonate; dibenzoyl peroxide;
In
tetrachloromethane; ethanol; N,N-dimethyl-formamide; toluene;
1: |Suzuki Coupling;
DOI:10.1039/c3cc48618d