C₃₈H₅₂O₈Si

Base Information

Chemical Name:C₃₈H₅₂O₈Si
CAS No.:781668-60-8
Molecular Formula:C₃₈H₅₂O₈Si
Molecular Weight:664.912
Hs Code.:

C<sub>38</sub>H<sub>52</sub>O<sub>8</sub>Si

Synonyms:C₃₈H₅₂O₈Si

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Chemical Property of C₃₈H₅₂O₈Si

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Technology Process of C₃₈H₅₂O₈Si

There total 8 articles about C₃₈H₅₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 781668-39-1
C₄₄H₆₆O₈Si₂

: 781668-60-8
C₃₈H₅₂O₈Si

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; pyridine; at 0 ℃; for 2h;
DOI:10.1002/anie.200460695

Reference yield:

: 781668-58-4
C₄₁H₆₂O₇Si₂

: 781668-60-8
C₃₈H₅₂O₈Si

Guidance literature:: Multi-step reaction with 4 steps

1: 4-DMAP; pyridine / CH₂Cl₂ / 3 h / 0 °C

2: LDA; HMPA; TBSCl / tetrahydrofuran / 72 h / -78 - 25 °C

3: 180 mg / DCC; 4-DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

4: 85 percent / HF*pyridine; pyridine / tetrahydrofuran / 5 h / 0 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; pyridine hydrogenfluoride; tert-butyldimethylsilyl chloride; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 2: Ireland-Claisen rearrangement;
DOI:10.1021/ja054750q

Reference yield:

: 781668-35-7
C₃₉H₅₈O₇Si₂

: 781668-60-8
C₃₈H₅₂O₈Si

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether; tetrahydrofuran / 1 h / 0 - 25 °C

2: 4-DMAP; pyridine / CH₂Cl₂ / 3 h / 0 °C

3: LDA; HMPA; TBSCl / tetrahydrofuran / 72 h / -78 - 25 °C

4: 180 mg / DCC; 4-DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

5: 85 percent / HF*pyridine; pyridine / tetrahydrofuran / 5 h / 0 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; pyridine hydrogenfluoride; tert-butyldimethylsilyl chloride; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; 3: Ireland-Claisen rearrangement;
DOI:10.1021/ja054750q