8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

Base Information

Chemical Name:8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane
CAS No.:1293374-99-8
Molecular Formula:C₂₃H₃₃ClO₂
Molecular Weight:376.967
Hs Code.:

Synonyms:8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

Chemical Property:

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Technology Process of 8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

There total 4 articles about 8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 51371-15-4
8β-hydroxypodocarpan-13-one

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 1293374-99-8
8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

Guidance literature:: (4-chlorphenyl)magnesium bromide; With cerium(III) chloride; In tetrahydrofuran; at 0 ℃; for 1.5h;

8β-hydroxypodocarpan-13-one; In tetrahydrofuran; at 0 - 20 ℃; for 9h;
DOI:10.3184/174751911X556701

Reference yield:

: 596-85-0
manool

: 1293374-99-8
8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium chlorochromate / dichloromethane

2.1: ozone / dichloromethane / -78 °C

3.1: sodium hydride / tetrahydrofuran / 4 h / Inert atmosphere

4.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / 0 °C

4.2: 9 h / 0 - 20 °C

With cerium(III) chloride; sodium hydride; ozone; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.3184/174751911X556701

Reference yield:

: 16633-27-5
(5S,9S,10S)-labda-8⁽¹⁷⁾,13-diene-15-al

: 1293374-99-8
8β,13β-dihydroxy-13α-4'-chlorophenylpodocarpane

Guidance literature:: Multi-step reaction with 3 steps

1.1: ozone / dichloromethane / -78 °C

2.1: sodium hydride / tetrahydrofuran / 4 h / Inert atmosphere

3.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / 0 °C

3.2: 9 h / 0 - 20 °C

With cerium(III) chloride; sodium hydride; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.3184/174751911X556701