(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

Base Information

Chemical Name:(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone
CAS No.:1374849-85-0
Molecular Formula:C₂₁H₂₀ClN₃O₂
Molecular Weight:381.862
Hs Code.:

Synonyms:(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

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Chemical Property of (R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

Chemical Property:

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Technology Process of (R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

There total 5 articles about (R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374849-88-3
C₁₂H₁₆ClN

: 98591-61-8
2-hydroxyquinoxaline-3-carbonyl chloride

: 1374849-85-0
(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 270596-39-9
Boc-(S)-3-amino-4-(3-chlorophenyl)butyric acid

: 1374849-85-0
(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3.2: 0.5 h / 0 - 20 °C

4.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

With hydrogenchloride; dmap; lithium aluminium tetrahydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1374849-86-1
C₁₇H₂₀ClNO₄

: 1374849-85-0
(R)-(2-(3-chlorobenzyl)piperidin-1-yl)(3-hydroxyquinoxalin-2-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 1,4-dioxane / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2.2: 0.5 h / 0 - 20 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane;