tris(m-aminophenyl)boroxine

Base Information

• Chemical Name: tris(m-aminophenyl)boroxine
• CAS No.: 151140-24-8
• Molecular Formula: C₁₈H₁₈B₃N₃O₃
• Molecular Weight: 356.792
• Mol file: 151140-24-8.mol

Synonyms:tris(m-aminophenyl)boroxine

Chemical Property of tris(m-aminophenyl)boroxine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of tris(m-aminophenyl)boroxine

There total 1 articles about tris(m-aminophenyl)boroxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Aminophenylboronic acid (30418-59-8,280563-63-5) → tris(m-aminophenyl)boroxine (151140-24-8)

Guidance literature:

at 110 ℃;

DOI:10.3762/bjoc.15.250

Reference yield: 10.0%

tris(m-aminophenyl)boroxine (151140-24-8) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6) → tricarbonyl(η(6)-aniline)chromium(0) (12108-11-1)

Guidance literature:

In tetrahydrofuran; dibutyl ether; (under N2); ratio aryl-compd.:Cr(CO)6 1:1, reflux for 24 h in Bu2O-THF; removal of the solvents, sublimation of the residue;

DOI:10.1016/0022-328X(93)80378-O

upstream raw materials:

3-Aminophenylboronic acid

Downstream raw materials:

tricarbonyl(η(6)-aniline)chromium(0)