Technology Process of 3-benzyloxy-1-adamantyl methyl ketone
There total 4 articles about 3-benzyloxy-1-adamantyl methyl ketone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H22O3; methyllithium;
In
diethyl ether;
at 0 - 20 ℃;
for 4.5h;
Inert atmosphere;
With
hydrogenchloride;
In
diethyl ether; water;
Inert atmosphere;
Cooling with ice;
DOI:10.1246/cl.2012.780
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: water; potassium hydroxide / ethanol / 2 h / Inert atmosphere; Reflux
2.1: diethyl ether / 4.5 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere; Cooling with ice
With
water; potassium hydroxide;
In
diethyl ether; ethanol;
DOI:10.1246/cl.2012.780
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2.1: water; potassium hydroxide / ethanol / 2 h / Inert atmosphere; Reflux
3.1: diethyl ether / 4.5 h / 0 - 20 °C / Inert atmosphere
3.2: Inert atmosphere; Cooling with ice
With
water; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium hydroxide;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1246/cl.2012.780
