Technology Process of C62H81BN6O14S4
There total 6 articles about C62H81BN6O14S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
ethanol;
at 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1002/chem.201103613
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethylmagnesium bromide / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere
1.2: 0.25 h / 60 °C / Inert atmosphere
2.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 60 °C / Inert atmosphere
3.1: N,N-dimethyl-formamide / 12 h / 60 °C / Inert atmosphere
4.1: water; sodium hydroxide / ethanol / 10 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; ethylmagnesium bromide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103613
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 60 °C / Inert atmosphere
2: N,N-dimethyl-formamide / 12 h / 60 °C / Inert atmosphere
3: water; sodium hydroxide / ethanol / 10 h / 20 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; water; triethylamine; sodium hydroxide;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103613