7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

Base Information

Chemical Name:7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane
CAS No.:226936-37-4
Molecular Formula:C₂₈H₃₄N₂O₅
Molecular Weight:478.588
Hs Code.:

Synonyms:7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

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Chemical Property of 7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

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Technology Process of 7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

There total 4 articles about 7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 226936-31-8
7,13-bis<4-(1-oxo-2-phenylselenylpropyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

: 226936-37-4
7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

Guidance literature:: With sodium periodate; sodium hydrogencarbonate; In tetrahydrofuran; methanol; water; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4020(99)00167-2

Reference yield:

: 456-03-1
1-(4-fluorophenyl)propan-1-one

: 226936-37-4
7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / tetrabutylammonium fluoride trihydrate / 12 h / 150 °C

2: 1.) LDA / 1) THF, heptane, -78 deg C, 1 h; 2) THF, heptane, 0 deg C, 2 h

3: 72 percent / NaHCO₃, NaIO₄ / tetrahydrofuran; methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; water;
DOI:10.1016/S0040-4020(99)00167-2

Reference yield:

: 31249-95-3
Kryptofix 21

: 226936-37-4
7,13-bis<4-(1-oxo-2-propenyl)phenyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / tetrabutylammonium fluoride trihydrate / 12 h / 150 °C

2: 1.) LDA / 1) THF, heptane, -78 deg C, 1 h; 2) THF, heptane, 0 deg C, 2 h

3: 72 percent / NaHCO₃, NaIO₄ / tetrahydrofuran; methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; water;
DOI:10.1016/S0040-4020(99)00167-2