Technology Process of C16H19FN4O5S
There total 8 articles about C16H19FN4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
at 0 - 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 3 h / 80 °C
1.2: 20 °C
2.1: hydrogenchloride / water; acetone / 1 h / 20 °C
3.1: hydroxylamine hydrochloride; sodium acetate / methanol / 0.5 h / Heating / reflux
4.1: triethylamine / dichloromethane / 20 °C
5.1: tetrahydrofuran / 0 - 20 °C
5.2: 4 h / 0 - 20 °C
6.1: diethyl ether / 0.5 h / 0 - 20 °C
7.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 0 - 20 °C
With
hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether / 0.5 h / 0 - 20 °C
2: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 0 - 20 °C
With
3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; chloroform;