3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde

Base Information

• Chemical Name: 3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde
• CAS No.: 868227-39-8
• Molecular Formula: C₃₂H₄₆O₅
• Molecular Weight: 510.714

Synonyms:3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde

Chemical Property of 3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde

Chemical Property:

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Safty Information:

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Technology Process of 3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde

There total 1 articles about 3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-((2E,6E,10E)-12-(2,3-bis(benzyloxy)-5-(1,3-dioxolan-2-yl)phenyl)-6,10-dimethyl-2-(4-methylpent-3-enyl)dodeca-2,6,10-trienyloxy)tetrahydro-2H-pyran (868227-38-7) → 3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde (868227-39-8)

Guidance literature:

With sodium; In iso-butanol; at 75 - 80 ℃; for 2.16667h;

DOI:10.1021/np050237e

Reference yield: 76.0%

3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde (868227-39-8) → 3,4-dihydroxy-5-((2E,6E,10E)-11-(hydroxymethyl)-3,7,15-trimethylhexadeca-2,6,10,14-tetraenyl)benzaldehyde (868227-40-1)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; for 3.5h;

DOI:10.1021/np050237e

Reference yield: 72.0%

3,4-dihydroxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde (868227-39-8) + acetic anhydride (108-24-7) → 3,4-diacetoxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde (868227-42-3)

Guidance literature:

With dmap; molecular sieve; diisopropylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/np050237e

upstream raw materials:

2-((2E,6E,10E)-12-(2,3-bis(benzyloxy)-5-(1,3-dioxolan-2-yl)phenyl)-6,10-dimethyl-2-(4-methylpent-3-enyl)dodeca-2,6,10-trienyloxy)tetrahydro-2H-pyran

Downstream raw materials:

3,4-dihydroxy-5-((2E,6E,10E)-11-(hydroxymethyl)-3,7,15-trimethylhexadeca-2,6,10,14-tetraenyl)benzaldehyde

3,4-diacetoxy-5-((2E,6E,10E)-3,7,15-trimethyl-11-((tetrahydro-2H-pyran-2-yloxy)methyl)hexadeca-2,6,10,14-tetraenyl)benzaldehyde

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