Technology Process of 3-ethyl-6-methoxy-7-(2'-carbomethoxy-6'-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene
There total 4 articles about 3-ethyl-6-methoxy-7-(2'-carbomethoxy-6'-methoxybenzoyl)-1,2,3,4-tetrahydronaphthalene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: BF3*Et2O / 2 h / 20 °C
1.2: 65 percent / sodium acetate / methanol / 4 h / Heating
2.1: 60 percent / HCl; hydrogen / 10 percent Pd/C / H2O; methanol / 8 h / 2585.74 Torr
3.1: 77 percent / zinc; mercuric chloride; HCl / toluene; H2O / 12 h / Heating
4.1: 70 percent / aluminium chloride / CH2Cl2 / 0 - 20 °C
With
hydrogenchloride; aluminium trichloride; boron trifluoride diethyl etherate; hydrogen; mercury dichloride; zinc;
palladium on activated charcoal;
In
methanol; dichloromethane; water; toluene;
3.1: Clemensen's reduction / 4.1: Friedel-Crafts acylation;
DOI:10.1016/S0040-4020(02)00740-8
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / HCl; hydrogen / 10 percent Pd/C / H2O; methanol / 8 h / 2585.74 Torr
2: 77 percent / zinc; mercuric chloride; HCl / toluene; H2O / 12 h / Heating
3: 70 percent / aluminium chloride / CH2Cl2 / 0 - 20 °C
With
hydrogenchloride; aluminium trichloride; hydrogen; mercury dichloride; zinc;
palladium on activated charcoal;
In
methanol; dichloromethane; water; toluene;
2: Clemensen's reduction / 3: Friedel-Crafts acylation;
DOI:10.1016/S0040-4020(02)00740-8