1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

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Chemical Name:1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide
CAS No.:503612-80-4
Molecular Formula:C₂₄H₂₄N₆O₄
Molecular Weight:460.492
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

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Chemical Property of 1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

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Technology Process of 1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

There total 3 articles about 1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: C₃₄H₃₃N₅O₇

: 503612-80-4
1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

Guidance literature:: C₃₄H₃₃N₅O₇; With palladium 10% on activated carbon; hydrogen; for 24h; under 2068.65 Torr;

With ammonia; In ethylene glycol; at 80 ℃; for 1.5h; Sealed tube;

Reference yield:

: 473927-64-9
1-(4-methoxy-phenyl)-6-(4-iodo-phenyl)-7-oxo-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxylic acid ethyl ester

: 503612-80-4
1-(4-methoxyphenyl)-7-oxo-6-[4-(2-oxo-1-piperazinyl)phenyl]-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 18 h / 130 °C / Inert atmosphere

2.1: hydrogen; palladium 10% on activated carbon / 24 h / 2068.65 Torr

2.2: 1.5 h / 80 °C / Sealed tube

With copper(l) iodide; palladium 10% on activated carbon; hydrogen; potassium carbonate; In dimethyl sulfoxide;