trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone

Base Information

• Chemical Name: trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone
• CAS No.: 82464-01-5
• Molecular Formula: C₂₇H₂₆N₂O₆
• Molecular Weight: 474.513

Synonyms:trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone

Chemical Property of trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone

Chemical Property:

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Technology Process of trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone

There total 1 articles about trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4b,10bβ,11,12-tetrahydro-4bβ,12β-(N-phenylepoxyimino)oxychelerythrine (67258-01-9,82534-85-8) → trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone (82464-01-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 0.25h; Ambient temperature;

DOI:10.1248/cpb.30.569

Reference yield: 74.0%

trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone (82464-01-5) → 2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,4-dihydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene (82464-00-4)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 0.333333h; Heating;

DOI:10.1248/cpb.30.569

Reference yield: 44.0%

trans-4-anilino-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-6,7-methylenedioxy-α-tetralone (82464-01-5) → cis-4-anilino-trans-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,2,3,4-tetrahydro-1-hydroxy-6,7-methylenedioxynaphthalene (82464-02-6,82509-32-8) + trans-4-anilino-cis-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,2,3,4-tetrahydro-1-hydroxy-6,7-methylenedioxynaphthalene (82464-02-6,82509-32-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 0.333333h; Ambient temperature;

DOI:10.1248/cpb.30.569

upstream raw materials:

4b,10bβ,11,12-tetrahydro-4bβ,12β-(N-phenylepoxyimino)oxychelerythrine

Downstream raw materials:

2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,4-dihydro-6,7-methylenedioxy-1-oxo-4-phenyliminonaphthalene

cis-4-anilino-trans-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,2,3,4-tetrahydro-1-hydroxy-6,7-methylenedioxynaphthalene

trans-4-anilino-cis-2-3',4'-dimethoxy-2'-methylcarbamoylphenyl-1,2,3,4-tetrahydro-1-hydroxy-6,7-methylenedioxynaphthalene

6-3',4'-dimethoxy-2'-methylcarbamoylphenyl-2,3-methylenedioxynaphthalene

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