5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

Base Information

Chemical Name:5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester
CAS No.:1448336-61-5
Molecular Formula:C₁₄H₁₃ClN₂O₃
Molecular Weight:292.722
Hs Code.:

Synonyms:5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

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Chemical Property of 5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

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Technology Process of 5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

There total 1 articles about 5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39891-09-3
(6-chloro-pyridin-3-yl)-acetonitrile

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1448336-61-5
5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1448336-61-5
5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

: 1448336-62-6
1-(6-chloro-pyridin-3-yl)-4-oxo-cyclohexanecarbonitrile

Guidance literature:: With lithium chloride; In dimethyl sulfoxide; at 120 ℃; for 2h; Microwave irradiation;

Reference yield:

: 1448336-61-5
5-cyano-5-(6-chloropyridin-3-yl)-2-oxocyclohexanecarboxylic acid methyl ester

: 1448336-63-7
1-(6-chloro-pyridin-3-yl)-4,4-difluoro-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: lithium chloride / dimethyl sulfoxide / 2 h / 120 °C / Microwave irradiation

2: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -78 °C

With diethylamino-sulfur trifluoride; lithium chloride; In dichloromethane; dimethyl sulfoxide;