C₆₀H₉₁N₉O₁₅

Base Information

Chemical Name:C₆₀H₉₁N₉O₁₅
CAS No.:1333408-31-3
Molecular Formula:C₆₀H₉₁N₉O₁₅
Molecular Weight:1178.43
Hs Code.:

C<sub>60</sub>H<sub>91</sub>N<sub>9</sub>O<sub>15</sub>

Synonyms:C₆₀H₉₁N₉O₁₅

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Chemical Property of C₆₀H₉₁N₉O₁₅

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Technology Process of C₆₀H₉₁N₉O₁₅

There total 11 articles about C₆₀H₉₁N₉O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1333408-34-6
C₁₈H₃₁N₃O₅

: 1333408-35-7
C₄₂H₆₂N₆O₁₁

: 1333408-31-3
C₆₀H₉₁N₉O₁₅

Guidance literature:: C₄₂H₆₂N₆O₁₁; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.0833333h; Inert atmosphere;

C₁₈H₃₁N₃O₅; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1007/s00726-011-0912-4

Reference yield:

benzyl (1S,3R)-3-acetyl-2,2-dimethylcyclobutyl-1-carbamate: 1017279-96-7
benzyl (1S,3R)-3-acetyl-2,2-dimethylcyclobutyl-1-carbamate

: 1333408-31-3
C₆₀H₉₁N₉O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hypobromide / 1,4-dioxane; water

2.1: caesium carbonate / N,N-dimethyl-formamide

3.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

6.2: 2 h / 20 °C / Inert atmosphere

With sodium hypobromide; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium formate; caesium carbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1007/s00726-011-0912-4

Reference yield:

(1R,3S)-3-(((benzyloxy)carbonyl)amino)-2,2-dimethylcyclobutan-1-carboxylic acid: 1017279-76-3
(1R,3S)-3-(((benzyloxy)carbonyl)amino)-2,2-dimethylcyclobutan-1-carboxylic acid

: 1333408-31-3
C₆₀H₉₁N₉O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide

2.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium formate; caesium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s00726-011-0912-4