methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:247092-74-6
Molecular Formula:C₃₅H₄₂Cl₃NO₁₃
Molecular Weight:791.076
Hs Code.:

Synonyms:methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 1 articles about methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 69558-07-2
methyl-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 161545-19-3
3,4,6-tri-O-acetyl-2-deoxy-2-trichloroacetamido-α/β-D-glucopyranose trichloroacetimidate

: 247092-74-6
methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃; for 15h;
DOI:10.1080/07328309908544033

Reference yield:

: 247092-74-6
methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 441777-52-2
methyl (2-amino-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 17h;
DOI:10.1016/S0040-4020(02)00148-5

Reference yield:

: 247092-74-6
methyl (3,4,6-tri-O-acetyl-2-trichloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: methyl (2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-O-benzyl-α-L-rhamnopyranoside

: methyl (3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->2)-3,4-di-O-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In N,N-dimethyl acetamide; toluene; at 100 ℃; for 0.75h;
DOI:10.1016/S0040-4020(02)00148-5