Technology Process of C74H102N8O8
There total 4 articles about C74H102N8O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27H44N2O4;
With
N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
N1,N3-bis(6-aminopyridin-2-yl)isophthalamide;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 12h;
DOI:10.1039/c1ob06026k
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 12 h / 50 °C
2.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 12 h / 50 °C
With
lithium hydroxide monohydrate; water; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06026k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C
2.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 12 h / 50 °C
3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 12 h / 50 °C
With
lithium hydroxide monohydrate; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06026k
