Technology Process of dimethyl 4-(6-butoxynaphthalene-2-sulfonamido)isophthalate
There total 6 articles about dimethyl 4-(6-butoxynaphthalene-2-sulfonamido)isophthalate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: thionyl chloride / 48 h / 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / methanol / 10 h / 20 °C
3: pyridine; triethylamine / dichloromethane / 48 h / 50 °C / Inert atmosphere
With
pyridine; thionyl chloride; palladium 10% on activated carbon; hydrogen; triethylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.04.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(I) oxide; copper; potassium carbonate / 2-ethoxy-ethanol / 0.75 h / 130 °C / Microwave irradiation; Inert atmosphere
2: thionyl chloride / 48 h / 20 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / methanol / 10 h / 20 °C
4: pyridine; triethylamine / dichloromethane / 48 h / 50 °C / Inert atmosphere
With
pyridine; copper(I) oxide; thionyl chloride; palladium 10% on activated carbon; hydrogen; copper; potassium carbonate; triethylamine;
In
methanol; 2-ethoxy-ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.04.011
