Technology Process of benzyl (5-cyclohexylidene-2,2-diphenyl-4-pentenyl)-carbamate
There total 7 articles about benzyl (5-cyclohexylidene-2,2-diphenyl-4-pentenyl)-carbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
ethanol; water;
at 23 ℃;
DOI:10.1021/ol071108n
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / dimethylformamide; tetrahydrofuran / cooling
1.2: 70 percent / sodium iodide / dimethylformamide; tetrahydrofuran / cooling
2.1: DIBAL-H / toluene; diethyl ether / cooling
2.2: sodium borohydride / toluene; diethyl ether; ethanol / cooling
3.1: sodium hydrogen carbonate / ethanol; H2O / 23 °C
With
sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol071108n
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: DIBAL-H / toluene; diethyl ether / cooling
1.2: sodium borohydride / toluene; diethyl ether; ethanol / cooling
2.1: sodium hydrogen carbonate / ethanol; H2O / 23 °C
With
diisobutylaluminium hydride; sodium hydrogencarbonate;
In
diethyl ether; ethanol; water; toluene;
DOI:10.1021/ol071108n
